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Aluminum Chloride Aluminium Chloride Hexahydrate BP USP Pure Manufacturers
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Specifications of Aluminum Chloride Anhydrous Manufacturers
MSDS of Aluminum Chloride Anhydrous Manufacturers
Aluminium Chloride Hexahydrate Commercial Pure
Aluminium Chloride Hexahydrate Grade 1
AlCl3·6H2O 241.43
[CAS 7784-13-6].
Assay: 98% minimum AlCl3 on dry basis.
Water: between 42.0% and 48.0%.
Sulfate— The addition of 0.2 mL of barium chloride TS to 10 mL of a solution (1 in 100) produces no turbidity within 1 minute.
Limit of alkalies and alkaline earths— To a boiling solution of 1.0 g in 150 mL of water add a few drops of methyl red TS, then add 6 N ammonium hydroxide until the color of the solution just changes to a distinct yellow. Add hot water to restore the volume to 150 mL, and filter while hot.
Evaporate 75 mL of the filtrate to dryness, and ignite to constant weight: the weight of the residue does not exceed 2.5 mg (0.5%).
Heavy metals, Method — the limit is 0.002%.
Iron — 0.001%.Aluminium Chloride Hexahydrate BP Ph Eur Specifications
DEFINITION
Content: 95.0 per cent to 101.0 per cent.
CHARACTERS
Appearance: White or slightly yellow, crystalline powder or colourless crystals, deliquescent.
Solubility: Very soluble in water, freely soluble in ethanol (96 per cent), soluble in glycerol.IDENTIFICATION
A. Dilute 0.1 ml of solution S2 (see Tests) to 2 ml with water R. The solution gives reaction (a) of chlorides.
B. Dilute 0.3 ml of solution S2 to 2 ml with water R. The solution gives the reaction of aluminium.TESTS
Solution S1: Dissolve 10.0 g in distilled water and dilute to 100 ml with the same solvent.
Solution S2: Dilute 50 ml of solution S1 to 100 ml with water.
Appearance of solution: Solution S2 is clear and not more intensely coloured than reference solution B7.
Sulphates: Maximum 100 ppm, determined on solution S1.
Iron: Maximum 10 ppm, determined on solution S1.
Alkali and alkaline-earth metals: Maximum 0.5 per cent.
To 20 ml of solution S2 add 100 ml of water and heat to boiling. To the hot solution add 0.2 ml of methyl red solution. Add dilute ammonia until the colour of the indicator changes to yellow and dilute to 150 ml with water. Heat to boiling and filter. Evaporate 75 ml of the filtrate to dryness on a water-bath and ignite to constant mass. The residue weighs a maximum of 2.5 mg.
Heavy metals: Maximum 20 ppm.
12 ml of solution S1 complies with test A. Prepare the reference solution using lead standard solution (2 ppm Pb).
Water: 42.0 per cent to 48.0 per cent, determined on 50.0 mg.
ASSAY
Dissolve 0.500 g in 25.0 ml of water R. Carry out the complexometric titration of aluminium. Titrate with 0.1 M zinc sulphate until the colour of the indicator changes from greyish green to pink. Carry out a blank titration.
1 ml of 0.1 M sodium edetate is equivalent to 24.14 mg of AlCl3,6H2O.For original monograph, please check the website of the relevant pharmacopoeia.
Aluminum Chloride USP Grade Specifications
AlCl3·6H2O -- 241.43 -- CAS 7784-13-6
Aluminum Chloride contains not less than 95.0 percent and not more than 102.0 percent of AlCl3, calculated on the anhydrous basis.
Identification: A solution (1 in 10) responds to the tests for Aluminum and for Chloride.
Water: Between 42.0% and 48.0%.
Sulfate: The addition of 0.2 mL of barium chloride to 10 mL of a solution (1 in 100) produces no turbidity within 1 minute.
Limit of alkalies and alkaline earths: the limit is 0.5%.
Heavy metals: the limit is 0.002%.
Iron: the limit is 0.001%.Aluminum Potassium Sulfate or Potash Alum
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Aluminium Chloride Hexahydrate Manufacturers
Aadhunik Industries
Ankleshwar Gujarat &, Mumbai, India
TEL: (OFFICE) 91-22-23774610, 23723564.e-mail: info@aadhunikindustries.com
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